Electrodeposited Au/FeAu Nanowires with Controlled Porosity

نویسندگان

  • S. Lucatero
  • W. H. Fowle
  • E. J. Podlaha
چکیده

Multilayer nanowires tailored with alternating AuFe porous layers and Au nonporous segments were fabricated by galvanic square-wave pulsed electrodeposition from a AuFe cyanide-free electrolyte. Control of porosity and composition was achieved via modulation in pulsed time and applied current density. Nanowires with decreased porosity were observed upon increasing time of the AuFe alloy layer or shifting the applied current density to more negative values. This transition was consistent with an increased amount of material being deposited. The single-step approach presented is less time-consuming than conventionally fabricated nanoporous materials, requiring additional etching of prefabricated solid alloys. © 2009 The Electrochemical Society. DOI: 10.1149/1.3238471 All rights reserved.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Influence of Citric and Ascorbic Acids on Electrodeposited Au/FeAu Multilayer Nanowires

AuFe electrodeposits onto a rotating disk electrode were examined to assess the composition and current efficiency behavior when citric acid, ascorbic acid, or a combination of both is present in the electrolyte. Nanowires were subsequently fabricated with pulsed current deposition to create compositionally, multilayered Au/FeAu nanowires. The FeAu layer of the nanowires was porous in a citrate...

متن کامل

Investigations of Magnetic Properties Through Electrodeposition Current and Controlled Cu Content in Pulse Electrodeposited CoFeCu Nanowires

CoFeCu nanowires were deposited by pulsed electrodeposition technique into the porous alumina templates by a two-step mild anodization technique, using the single-bath method. The electrodeposition was performed in a constant electrolyte while Cu constant was controlled by electrodeposition current. The electrodeposition current was 3.5, 4.25, 5 and 6 mA. The effect of electrodeposition current...

متن کامل

Investigations of Microstructures and Magnetic Properties through Off-time between Pulses and Controlled Cu Content in Pulse Electrodeposited NiCu Nanowires

NiCu alloy nanowires arrays were embedded into the anodic aluminum oxide (AAO) template by ac-pulse electrodeposition. Different off-time were used in electrolyte with constant concentration of Ni and Cu and acidity of 3. The effect of deposition parameters on alloy contents was investigated by studying the microstructure and magnetic properties of as-deposited NiCu alloy nanowires. Atomic forc...

متن کامل

Growth and morphological analysis of segmented AuAg alloy nanowires created by pulsed electrodeposition in ion-track etched membranes

BACKGROUND Multicomponent heterostructure nanowires and nanogaps are of great interest for applications in sensorics. Pulsed electrodeposition in ion-track etched polymer templates is a suitable method to synthesise segmented nanowires with segments consisting of two different types of materials. For a well-controlled synthesis process, detailed analysis of the deposition parameters and the siz...

متن کامل

Electrochemically fabricated zero-valent iron, iron-nickel, and iron-palladium nanowires for environmental remediation applications.

Monodisperse crystalline zero-valent iron, iron-nickel, iron-palladium nanowires were synthesised using template-directed electrodeposition methods. Prior to nanowire fabrication, alumina nanotemplates with controlled pore structure (e.g. pore diameter and porosity) were fabricated by anodising high purity aluminium foil in sulphuric acid. After fabrication of alumina nanotemplates, iron, iron-...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2009